Login| Sign Up| Help| Contact|

Patent Searching and Data


Title:
METHOD OF MANUFACTURING RARE-EARTH MAGNETIC MINUTE POWDER
Document Type and Number:
Japanese Patent JPH05308011
Kind Code:
A
Abstract:

PURPOSE: To manufacture a rare-earth magnetic minute powder without pulverizing an ingot or a ribbon material by a method wherein an aqueous solution of a salt of an iron group three-membered element and a rare-earth element is added to an aqueous solution containing a specific reducing agent.

CONSTITUTION: Chloride or sulfate of an iron group three-membered element (iron, cobalt, nickel) and a rare-earth element is added to an aqueous solution containing a reducing agent such as a hydroride of boron kalium, a hydroride of boron sodium, or the like and a reducing agent of dimethylamine boron, whereby a rare-earth magnetic minute powder can be made. For example, after an aqueous solution of a hydroride of boron kalium is dropped into an aqueous solution containing FeSO4, NdCl3, and dimethylamine boron, it is left as it is for 10min. and the Nd-Fe-B minute powder is separated out. After the separated matter is filtered through a glass filter, washed by distilled water, washed by methanol, and washed by acetone, it is dried under vacuum along with the glass filters. Incidentally, it is desired that the amount of the hydroride of boron kalium should be suppressed down to a half of the reaction conclusion amount or less which is calculated in an atoichiometry method.


Inventors:
WATANABE SHUNJI
SHISHIDO AKIYA
Application Number:
JP8428391A
Publication Date:
November 19, 1993
Filing Date:
April 16, 1991
Export Citation:
Click for automatic bibliography generation   Help
Assignee:
SEIKO INSTR INC
International Classes:
B22F9/24; H01F1/053; H01F1/057; H01F1/06; (IPC1-7): H01F1/06; B22F9/24; H01F1/053
Attorney, Agent or Firm:
Keinosuke Hayashi