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Title:
PRODUCTION OF PURE AND UNSYMMETRICALLY DI-SUBSTITUTED UREA
Document Type and Number:
Japanese Patent JPH03173860
Kind Code:
A
Abstract:

PURPOSE: To easily obtain the subject compound of high purity by reacting N-alkylamine or N,N-dialkylurea with substituted allyamine or heterocyclic amine, in the presence of the amine which is already present in the starting material can be obtained easily.

CONSTITUTION: N-alkylurea or N,N-dialkyurea of formula I (R1, R2 mean H, alkyl, wherein both R1 and R2 are not H or R1 and R2 may form together butylene, bentylene) are used as a starting material, and in the presence or absence of a diluent, by reacting said compound with amine of formulas II (R is unsubstituted or mono- or poly substituted phenyl by halogen, or alkyl, alkoxy, etc.; oxazoline, isooxazolyl, etc.), in the presence of amine in excess expressed by formula III, a compound of formula IV can be obtained. Preferably, dimethylurea is used as a compound of formula I, and dimethylamine is used as a compound of formula III.


Inventors:
RUUDORUFU HERUMUUTO UERUTOHERU
HORUSUTO KORUNTONAA
EGUMONTO AUERU
KURUTO TOONHOOFUERU
Application Number:
JP30125090A
Publication Date:
July 29, 1991
Filing Date:
November 08, 1990
Export Citation:
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Assignee:
AGURORINTSU AGURARUHIEMIKAARIN
International Classes:
C07C273/18; C07C275/28; C07C275/30; C07C275/32; C07C275/34; C07C275/36; C07D261/14; C07D263/48; C07D263/58; C07D277/48; C07D277/82; C07D277/20; (IPC1-7): C07C273/18; C07C275/28; C07C275/30; C07C275/32; C07C275/34; C07C275/36; C07D261/14; C07D263/48; C07D263/58; C07D275/03; C07D277/48; C07D277/82
Attorney, Agent or Firm:
Mitsuyoshi Esaki (3 outside)