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Patent Searching and Data


Title:
STABILE SOLUTION OF ACIDIC CRUMBS OF POLY(P-PHENYLENE TEREPHTHALAMIDE)
Document Type and Number:
Japanese Patent JPH02202522
Kind Code:
A
Abstract:

PURPOSE: To obtain a solution from which a fibrid product can be directly prepared by reacting terephthaloyl chloride with p-phenylenediamine in a specified solvent and adding e.g. potassium hydroxide and an auxiliary solvent comprising an alcohol to the reaction mixture under agitation.

CONSTITUTION: This solution is obtained by reacting terephthaloyl chloride with p-phenylenediamine by contact under agitation in an anhydrous solution containing an N-alkylpyrrolidone and at least one anhydrous alkali (alkaline earth) metal salt to form wet acidic crumbs of a polymer and adding 2.6-5.9 mol, per mol of the NH groups of the polymer, a base such as KOH, NaOH and a 5C or lower sodium or potassium alkoxide and 10.0-38.0 mol of a auxiliary solvent represented by the formula: X-OH (wherein X is H or a 5C or lower alkyl).


Inventors:
JIEIMUZU EDOMONDO BAN TORANPU
Application Number:
JP32071289A
Publication Date:
August 10, 1990
Filing Date:
December 12, 1989
Export Citation:
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Assignee:
DU PONT
International Classes:
D01F6/60; D21H13/26; C08G69/46; (IPC1-7): C08G69/46; D01F6/60; D21H13/26
Attorney, Agent or Firm:
Heiyoshi Odashima (1 person outside)