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Title:
METHOD OF PRODUCTION FOR TRIMETHYLOL PROPANE WITH LOW APHA COLOR NUMBER
Document Type and Number:
Japanese Patent JP2003192620
Kind Code:
A
Abstract:

To provide a method for production of trimethylol propane with low APHA (American Public Health Organization) color number, suitable for production of a resin for paint, powder paint, a foam or a polyester.

The method comprises a step a) forming a reaction mixture containing trimethylol propane by reacting n-butylaldhyde and/or 2,2-dimethylol butylaldehyde in the presence of formaldehyde and an inorganic base, a step b) at least partially removing water and an inorganic salt from the reaction mixture containing the trimethylol propane obtained in the step a) to obtain the crude trimethylol propane, and a step c) separating the crude trimethylol propane obtained in the step b) by distillation into a low-boiling fraction, a medium-boiling fraction containing at least one substance mainly comprising the trimethylol propane and a high-boiling fraction.


Inventors:
MUELLER DIRK
WAGNER PAUL
SCHWEGLER BRIAN
NOTHEIS ULRICH
ARMBRUST RALPH
HEINZ HANS-DETLEF
WAGNER ALEXANDER
Application Number:
JP2002373118A
Publication Date:
July 09, 2003
Filing Date:
December 24, 2002
Export Citation:
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Assignee:
BAYER AG
International Classes:
C07C29/36; C07B61/00; C07C29/38; C07C29/80; C07C31/22; (IPC1-7): C07C29/36; C07C29/80; C07C31/22
Attorney, Agent or Firm:
Toshio Yano (4 outside)